Nanotechnology Now

Our NanoNews Digest Sponsors





Heifer International

Wikipedia Affiliate Button


android tablet pc

Home > Press > Carbon Nanotube Measurements: Latest in NIST ‘How-To’ Series

Scanning electron microscope image of 'cleaned' carbon nanotubes at NIST (color added for clarity.)

Credit: NIST
Scanning electron microscope image of 'cleaned' carbon nanotubes at NIST (color added for clarity.)

Credit: NIST

Abstract:
The National Institute of Standards and Technology (NIST), in collaboration with the National Aeronautics and Space Administration (NASA), has published detailed guidelines* for making essential measurements on samples of single-walled carbon nanotubes (SWCNTs). The new guide constitutes the current "best practices" for characterizing one of the most promising and heavily studied of the new generation of nanoscale materials.

Carbon Nanotube Measurements: Latest in NIST ‘How-To’ Series

GAITHERSBURG, MD | Posted on April 15th, 2008

The nanotubes are essentially cylinders of carbon atoms with a wall only one atom thick and a diameter of a couple of nanometers—but lengths up to several million times their diameter. (Think of a soup can about 100 kilometers tall.) Because of their unique electronic, thermal, optical and mechanical properties they are being studied for a wide—and expanding—range of applications, including ultrastrong fibers for nanocomposite materials, circuit elements in molecular electronics, hydrogen storage components for fuel cells and light sources for compact, efficient flat-panel displays. One basic problem is assuring the quality and purity of SWCNT materials. All known techniques for producing these tiny tubes also produce large quantities of nanojunk: simple graphite and carbon soot often encapsulating small metal particles used to catalyze the nanotube synthesis process. (See, for example, "NIST Laser-Based Method Cleans Up Grubby Nanotubes", Tech Beat Dec. 1, 2006.)

Accurate, reliable and preferably rapid measurement techniques are needed to optimize production processes to create more product and less impurities. These will help to control cleaning and purifying processes and ultimately to improve the confidence of buyers and sellers of SWCNT materials. Beginning in 2003, NIST and NASA researchers started addressing the problem by sponsoring a series of workshops devoted to nanotube measurements. The NIST "Recommended Practice Guide" on Measurement Issues in Single Wall Carbon Nanotubes grew out of second workshop in 2005, and represents what industry, government and academic researchers regard as the most useful and accurate measurement techniques for characterizing the purity of SWCNT samples. The techniques discussed include thermogravimetric analysis; near-infrared spectroscopy; Raman spectroscopy and optical, electron and scanned probe microscopy. Researchers from the NASA Johnson Space Center, the University of California at Riverside, Boston University and the NASA Langley Research Center contributed to the guide.

The techniques described in the guide were proposed as the basis for international standards for nanotube characterization. A collaborative effort that includes the US, China, Japan, and Korea is now underway under the International Organization for Standardization (ISO) to develop these techniques into standards that will help ensure uniform characterization metrics used when buying and selling nanotubes. The editors caution that in the fast-moving field of carbon nanotubes, characterization methods will need to be updated periodically.

The NIST Recommend Practice Guides are a set of publications devoted to specific, challenging measurement issues faced in industry and research. Online copies of Measurement Issues in Single Wall Carbon Nanotubes and other guides in the series are available at The "How To Measure" Book Series.

* S. Freiman, S. Hooker, K. Migler and S. Arepalli (eds.). Measurement Issues in Single Wall Carbon Nanotubes. NIST Special Publication 960-19, March 2008.

####

About NIST
The National Institute of Standards and Technology (NIST) is a non-regulatory agency of the U.S. Department of Commerce. NIST promotes U.S. innovation and industrial competitiveness by advancing measurement science, standards and technology in ways that enhance economic security and improve our quality of life.

For more information, please click here

Contacts:
Michael Baum

(301) 975-2763

Copyright © NIST

If you have a comment, please Contact us.

Issuers of news releases, not 7th Wave, Inc. or Nanotechnology Now, are solely responsible for the accuracy of the content.

Bookmark:
Delicious Digg Newsvine Google Yahoo Reddit Magnoliacom Furl Facebook

Related News Press

Imaging

Detecting Cancer Earlier is Goal of Rutgers-Developed Medical Imaging Technology: Rare earth nanocrystals and infrared light can reveal small cancerous tumors and cardiovascular lesions October 21st, 2014

News and information

Detecting Cancer Earlier is Goal of Rutgers-Developed Medical Imaging Technology: Rare earth nanocrystals and infrared light can reveal small cancerous tumors and cardiovascular lesions October 21st, 2014

Nitrogen Doped Graphene Characterized by Iranian, Russian, German Scientists October 21st, 2014

Physicists build reversible laser tractor beam October 20th, 2014

Removal of Limitations of Composites at Superheat Temperatures October 20th, 2014

Govt.-Legislation/Regulation/Funding/Policy

Crystallizing the DNA nanotechnology dream: Scientists have designed the first large DNA crystals with precisely prescribed depths and complex 3D features, which could create revolutionary nanodevices October 20th, 2014

Imaging electric charge propagating along microbial nanowires October 20th, 2014

HP Supercomputer at NREL Garners Top Honor October 19th, 2014

First Canada Excellence Research Chair gets $10 million from the federal government for oilsands research at the University of Calgary: Federal government announces prestigious research chair to study improving oil production efficiency October 19th, 2014

Announcements

Detecting Cancer Earlier is Goal of Rutgers-Developed Medical Imaging Technology: Rare earth nanocrystals and infrared light can reveal small cancerous tumors and cardiovascular lesions October 21st, 2014

Nitrogen Doped Graphene Characterized by Iranian, Russian, German Scientists October 21st, 2014

Physicists build reversible laser tractor beam October 20th, 2014

Removal of Limitations of Composites at Superheat Temperatures October 20th, 2014

Tools

Detecting Cancer Earlier is Goal of Rutgers-Developed Medical Imaging Technology: Rare earth nanocrystals and infrared light can reveal small cancerous tumors and cardiovascular lesions October 21st, 2014

New Grand ARM Transmission Electron Microscope Offers Highest Commercially-Available Atomic Resolution of 63 Picometers October 17th, 2014

Nanodevices for clinical diagnostic with potential for the international market: The development is based on optical principles and provides precision and allows saving vital time for the patient October 15th, 2014

Unique catalysts for hydrogen fuel cells synthesized in ordinary kitchen microwave oven October 14th, 2014

NanoNews-Digest
The latest news from around the world, FREE





  Premium Products
NanoNews-Custom
Only the news you want to read!
 Learn More
NanoTech-Transfer
University Technology Transfer & Patents
 Learn More
NanoStrategies
Full-service, expert consulting
 Learn More














ASP
Nanotechnology Now Featured Books




NNN

The Hunger Project







© Copyright 1999-2014 7th Wave, Inc. All Rights Reserved PRIVACY POLICY :: CONTACT US :: STATS :: SITE MAP :: ADVERTISE